[1]符继红,高晶,唐军.气相色谱-质谱法测定不同品种薰衣草精油中 芳樟醇和乙酸芳樟酯的含量[J].中国调味品,2016,(10):97-100.[doi:10.3969/j.issn.1000-9973.2016.10.021]
 FU Ji-hong,GAO Jing,TANG Jun.Determination of Linalool and Linalyl Acetate in Different Varieties of Lavender Essential Oils Using Gas Chromatography-Mass Spectrometry[J].CHINA CONDIMENT,2016,(10):97-100.[doi:10.3969/j.issn.1000-9973.2016.10.021]
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气相色谱-质谱法测定不同品种薰衣草精油中 芳樟醇和乙酸芳樟酯的含量
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《中国调味品》[ISSN:1000-9973/CN:23-1299/TS]

卷:
期数:
2016年10期
页码:
97-100
栏目:
分析检测
出版日期:
1900-01-01

文章信息/Info

Title:
Determination of Linalool and Linalyl Acetate in Different Varieties of Lavender Essential Oils Using Gas Chromatography-Mass Spectrometry
文章编号:
1000-9973(2016)10-0097-04
作者:
符继红高晶唐军
新疆大学理化测试中心,乌鲁木齐 830046
Author(s):
FU Ji-hong GAO Jing TANG Jun
Physics and Chemistry Detecting Center, Xinjiang University, Urumqi 830046, China
关键词:
气相色谱-质谱联用 薰衣草精油 芳樟醇 乙酸芳樟酯
Keywords:
GC-MS lavender essential oil linalool linalyl acetate
分类号:
TS201.2
DOI:
10.3969/j.issn.1000-9973.2016.10.021
摘要:
采用水蒸气蒸馏法提取薰衣草精油,建立气相色谱-质谱联用(GC-MS)技术的检测方法,对新疆不同品种的薰衣草精油中芳樟醇和乙酸芳樟酯的含量进行了测定。芳樟醇和乙酸芳樟酯的线性范围分别为4.71~33.91 μg和5.00~21.49 μg,相关系数分别为0.9992和0.9991,相对标准偏差小于5%,平均回收率分别为94.67%和96.57%。测定了新疆主要种植的3个不同品种的15个薰衣草精油样品中芳樟醇和乙酸芳樟酯的含量,同时检测了不同品种薰衣草精油的提取率。结果表明:薰衣草精油中芳樟醇和乙酸芳樟酯含量的差异主要是由不同的品种造成的,其中芳樟醇在法国蓝精油中含量最高,乙酸芳樟酯在H-701精油中含量最高,并且不同品种薰衣草精油的提取率不同。所得数据可为薰衣草精油的进一步研究和开发利用提供科学依据。
Abstract:
An analytical method has been developed for the simultaneous determination of linalool and linalyl acetate in different varieties of lavender essential oils by gas chromatography/mass spectrometry(GC-MS). The essential oils are extracted from Lavandula angustifolia Mill.by steam distillation. The content of linalool and linalyl acetate is analyzed by GC-MS. The linear range of linalool and linalyl acetate is 4.71~33.91 μg and 5.00~21.49 μg, the correlation coefficient is 0.9992 and 0.9991 and the recoveries are 94.67% and 96.57% respectively. The relative standard deviation(RSD,%)is less than 5%. This method can be used for determination of linalool and linalyl acetate in lavender essential oils. Fifteen essential oil samples which belong to three different lavender species are analyzed by GC-MS collected in Xinjiang. The results show that the difference in content of linalool and linalyl acetate is mainly caused by different varieties. Linalool is found in the highest content in French blue and linalyl acetate is found in the highest content in H-701. The extraction rates of lavender essential oils are different. The obtained data have provided the scientific evidences for the further studies and utilization of lavender essential oils.

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备注/Memo

备注/Memo:
基金项目:国家自然科学基金(21565024); 新疆高校科研计划科学研究重点项目(XJEDU2012I14); 新疆大学博士科研启动基金(BS120135)
作者简介:符继红(1977-),女,副教授,博士,主要从事天然产物及食品分析的研究。
更新日期/Last Update: 1900-01-01